Practical experience with the ETV-ICP-MS prototype
ČlánekStatus neznámýpeer-reviewedpublishedDatum publikování
2019
Vedoucí práce
Oponent
Název časopisu
Název svazku
Vydavatel
University of Pardubice
Abstrakt
The aim of this study was to evaluate the commercial instrumental connection of the
electrothermal vaporization unit (ETV) GF 5000 and the inductively coupled plasma
orthogonal acceleration time-of-flight mass spectrometer (ICP-o-TOF-MS) Optimass
9500, both from the company GBC Scientific Equipment (Braeside, Australia). The
prototype of the ETV unit was borrowed by the manufacturer for the purpose of its
testing in the connection with the ICP-TOF-MS. Information on this technique
instrumental arrangement has not been found in the literature yet. Therefore, the facts
summarized in this paper are based mainly on our observations. The analytical
performance of this technique achieved in our previous work is discussed and compared
to competing spectrochemical methods. The attention was paid to the software and
technical shortcomings observed within three years of working with this configuration.
The influence of shortcomings of the instrument found during testing has been evaluated
from the point of view of potential analytical applicability in its entirety and with respect
to the economic impact on routine use.
Rozsah stran
p. 27 - 39
ISSN
1211-5541
Trvalý odkaz na tento záznam
Projekt
Zdrojový dokument
Scientific papers of the University of Pardubice. Series A, Faculty of Chemical Technology. 25/2019
Vydavatelská verze
Přístup k e-verzi
open access
Název akce
ISBN
978-80-7560-243-5
Studijní obor
Studijní program
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Klíčová slova
ETV-ICP-MS, user evaluation, software shortcomings, technical short-comings, switching valve, sample dosing monitoring