| dc.contributor.author |
Kačík, F.
|
cze |
| dc.contributor.author |
Podzimek, Štěpán
|
cze |
| dc.contributor.author |
Vizárová, K.
|
cze |
| dc.contributor.author |
Kačíková, D.
|
cze |
| dc.contributor.author |
Čabalová, I.
|
cze |
| dc.date.accessioned |
2017-05-11T11:14:04Z |
|
| dc.date.available |
2017-05-11T11:14:04Z |
|
| dc.date.issued |
2016 |
eng |
| dc.identifier.issn |
0969-0239 |
eng |
| dc.identifier.uri |
http://hdl.handle.net/10195/67632 |
|
| dc.description.abstract |
In this work, we compared three methods of analysis of cellulose in paper subjected to accelerated ageing: size exclusion chromatography in combination with multiangle light scattering (SEC-MALS) detection, size exclusion chromatography in combination with diode-array detector and calibration using polystyrene standards (SEC-DAD), and asymmetric flow field–flow fractionation in combination with multiangle light scattering (A4F-MALS). Prior to separation, cellulose sample were derivatized with phenyl isocyanate to CTC and dissolved in tetrahydrofuran. |
eng |
| dc.format |
p. 357-366 |
eng |
| dc.language.iso |
eng |
eng |
| dc.relation.ispartof |
Cellulose, volume 23, issue: 1 |
eng |
| dc.rights |
open access |
eng |
| dc.subject |
Cellulose |
eng |
| dc.subject |
Tricarbanilates (CTC) |
eng |
| dc.subject |
Degree of polymerization (DP) |
eng |
| dc.subject |
Size exclusion chromatography (SEC) |
eng |
| dc.subject |
Asymmetric flow field–flow fractionation (A4F |
eng |
| dc.subject |
Paper degradation |
eng |
| dc.subject |
Trikarbanilát celulózy (CTC) |
cze |
| dc.subject |
polymerační stupeň (DP) |
cze |
| dc.subject |
gelová permeační chromatografie (GPC) |
cze |
| dc.subject |
frakcionace tokem v asymetrickém tokovém poli (A4F) |
cze |
| dc.title |
Characterization of cellulose degradation during accelerated ageing by SEC-MALS, SEC-DAD, and A4F-MALS methods |
eng |
| dc.title.alternative |
Charakterizace degradace celulózy v průběhu urychleného stárnutí pomocí GPC-MALS, GPC-DAD a A4F-MALS |
cze |
| dc.type |
article |
eng |
| dc.description.abstract-translated |
Práce porovnává tři metody analýzy celulózy vystavené urychlenému stárnutí: gelová permeační chromatografie v kombinaci s víceúhlovým rozptylem světla (GPC-MALS), gelovou permeační chromatografii v kombinaci s detektorem diodového pole a kalibrací na polystyrenové standardy (GPC-DAD) a frakcionaci tokem v asymetrickém tokovém poli (A4F-MALS). Před separací byly vzorky derivatizovány fenyl izokyanátem na CTC a rozpuštěny v tetrahydrofuranu. |
cze |
| dc.peerreviewed |
yes |
eng |
| dc.publicationstatus |
postprint |
eng |
| dc.identifier.doi |
10.1007/s10570-015-0842-5 |
|
| dc.identifier.wos |
000368802700022 |
|
| dc.identifier.scopus |
2-s2.0-84955461413 |
|
| dc.identifier.obd |
39877591 |
eng |
