Studium vlivu složení plniva kompozitního systému na jeho emisivitu

Mauer, Milan

Publikace:
Studium vlivu složení plniva kompozitního systému na jeho emisivitu

Disertační práceopen access

dc.contributor.author	Mauer, Milan
dc.contributor.referee	Martan, Jiří
dc.contributor.referee	Ventura, Karel
dc.date.accepted	2017-11-21
dc.date.accessioned	2017-12-04T07:14:59Z
dc.date.available	2017-12-04T07:14:59Z
dc.date.issued	2017
dc.date.submitted	2017-09-20
dc.description.abstract	Byla studována možnost ovlivnit emisivní vlastnosti keramického kompozitu pouho změnou složení plniv. Cílem bylo najít takové složení plniv, které bude mít velmi vysokou emisivitu (> 0.90) a to i za teplot, ve kterých operují tepelná zařízení. Následně bylo nutné provést porovnávací testy mezi původní recepturou a nově vyvinutým emisivním materiálem (teplotní odolnost, tepelná vodivost, přilnavost a SEM analýzy vzorků vypalených při různých teplotách).	cze
dc.description.abstract-translated	The research work is focused on the possibility to influence the emissivity of an inorganic composite coating by changing the filler composition. These coatings can also be used in power-producing equipment and they can increase the efficiency of this type of equipment thanks to high emissivity. The intention of our project is to develop a system which will provide a very high normal spectral emissivity (0.75 - 0.99) within a short and medium wavelength range of infrared spectrum of electromagnetic radiation (1,5 ? 8,0 ?m) and at temperatures above 700 oC where most of the thermal energy is transfered. For example lining materials usually have the emissivity of 0.20 ? 0.40 in this spectral zone, steel has the emissivity of 0.60 ? 0.80. This provides sufficient space for the emissivity improvement by the developed emissivity coatings. The coatings have to be resistant to the given conditions which occure in the thermal equipments (very high temperature and different level of abrasion). BG HitCoat? is one of these protective coatings. Chromium Oxide is the active ingredient which is contained in the filler of its basic composition. Other active ingredients were also built into the matrix of the composite. Some of the active ingredients had high value of emissivity (Iron, Silicon Carbide), others had high value of melting temperature (Magnezite, Magnetite, Kaolin, Boron Carbide, Boron Nitride, Zirconium Oxide, etc.). Emissivity comparison of new samples then followed. Fourrier Transform Infra-Red (FTIR) Spectrometry was applied for measurement of normal spectral emissivity. Research required measurements carried out mainly at high temperatures. Radiation of researched materials was compared with radiation of the comparative high temperature coating based on Cr2O3 and with radiation of the black body. Influence of filler composition on the emissivity in monitored range of infrared spectrum was demonstrated. The least emissive active ingredient (Zirconium Oxide) had the values of 0.09 ? 0.60 in the range, the most emissive one (mixture of nitrides) had the values of 0,75 - 0,93. The material with the most emissive active ingredient was then subjected to comparison with the original formulation. All important parameters were compared (thermal resistance, thermal conductivity, adhesion, morphology) and the new material was comparable in all the tests.	eng
dc.description.department	Fakulta chemicko-technologická	cze
dc.description.grade	Dokončená práce s úspěšnou obhajobou	cze
dc.format	106 s.
dc.identifier	Univerzitní knihovna (studovna)
dc.identifier.signature	D37171
dc.identifier.stag	34742
dc.identifier.uri	https://hdl.handle.net/10195/69677
dc.language.iso	cze
dc.publisher	Univerzita Pardubice	cze
dc.rights	bez omezení	cze
dc.subject	anorganické kompozity	cze
dc.subject	IČ spektrometrie	cze
dc.subject	emisivita	cze
dc.subject	inorganic composites	eng
dc.subject	IR spectrometry	eng
dc.subject	emissivity	eng
dc.thesis.degree-discipline	Povrchové inženýrství	cze
dc.thesis.degree-grantor	Univerzita Pardubice. Fakulta chemicko-technologická	cze
dc.thesis.degree-name	Ph.D.
dc.thesis.degree-program	Chemie a technologie materiálů	cze
dc.title	Studium vlivu složení plniva kompozitního systému na jeho emisivitu	cze
dc.title.alternative	Study of influence of filler compositionin in composite systems on emissivity	eng
dc.type	disertační práce	cze
dspace.entity.type	Publication