Preparation of porcupine-like Bi2O3 needle bundles by anodic oxidation of bismuth

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dc.contributor.author Sopha, Hanna
dc.contributor.author Podzemná, Veronika
dc.contributor.author Hromádko, Luděk
dc.contributor.author Macák, Jan
dc.date.accessioned 2017-10-02T07:04:44Z
dc.date.available 2017-10-02T07:04:44Z
dc.date.issued 2017-09-18
dc.identifier.issn 1388-2481
dc.identifier.uri https://hdl.handle.net/10195/69562
dc.description.abstract A new Bi2O3 structure resembling bundles of needles was prepared by anodic oxidation of a bismuth substrate in H2SO4 electrolyte followed by annealing in air. Needle growth occurred on the timescale of minutes. The resulting porcupine-like needle bundles were characterized using SEM and XRD before and after annealing. The as-grown needles consisted of bismuth aqua sulfate hydroxide; however, upon annealing at 250 °C in air, tetragonal β-Bi2O3 was produced without any morphological change. cze
dc.format p. 6-9 eng
dc.language.iso en cze
dc.publisher Elsevier cze
dc.relation.ispartof Electrochemistry Communications. 2017, vol. 84
dc.rights Attribution-NonCommercial-NoDerivs 3.0 Czech Republic *
dc.rights.uri http://creativecommons.org/licenses/by-nc-nd/3.0/cz/ *
dc.subject Anodization cze
dc.subject bismuth cze
dc.subject bismuth oxide cze
dc.subject breakdown cze
dc.subject needles cze
dc.title Preparation of porcupine-like Bi2O3 needle bundles by anodic oxidation of bismuth cze
dc.type Article cze
dc.peerreviewed yes eng
dc.publicationstatus postprint eng
dc.identifier.doi 10.1016/j.elecom.2017.09.013
dc.relation.publisherversion http://www.sciencedirect.com/science/article/pii/S1388248117302576
dc.project.ID EC/H2020/638857/EU/Towards New Generation of Solid-State Photovoltaic Cell: Harvesting Nanotubular Titania and Hybrid Chromophores/CHROMTISOL
dc.identifier.scopus 2-s2.0-85029658288


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